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2007:
Murruzzu Caterina; Alonso Mònica; Canales Angeles; Jiménez-Barbero Jesus; Riera Antoni
Synthesis and NMR experiments of (4,5,6-13C)-deoxymannojirimycin. A new entry to 13C-labeled glycosidase inhibitors.
Carbohydrate research 2007;
342(
12-13):.
The synthesis of (4,5,6-13C)-deoxymannojirimycin is described. The route employed is based on Sharpless asymmetric epoxidation of (1,2,3-13C)(E)-2,4-pentadien-1-ol and uses ring-closing metathesis as a key step. The labeled compound may be easily used for protein-binding experiments using NMR spectroscopic methods.
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