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Roberto Cirilli

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Simone Carradori; Roberto Cirilli; Simona Dei Cicchi; Rosella Ferretti; Sergio Menta; Marco Pierini; Daniela Secci
3-methylcyclohexanone thiosemicarbazone: determination of E/Z isomerization barrier by dynamic high-performance liquid chromatography, configuration assignment and theoretical study of the mechanisms involved by the spontaneous, acid and base catalyzed processes.
dante rotili; Alberta Samuele; Domenico Tarantino; Ludovica Morera; Ira Musmuca; Maxim B Nawrozkij; Marco Pierini; Rino Ragno; Marino Artico; FLAVIO BALLANTE; Giorgia Botta; Roberto Cirilli; Bonaventura Clotet; José A Esté; Emmanuel Gonzalez; giovanni maga; Antonello Mai
2-(Alkyl/aryl)amino-6-benzylpyrimidin-4(3H)-ones as inhibitors of wild-type and mutant HIV-1: enantioselectivity studies.
Stefano Alcaro; Adriana Bolasco; Roberto Cirilli; Rosella Ferretti; Rossella Fioravanti; Francesco Ortuso
Computer-aided molecular design of asymmetric pyrazole derivatives with exceptional enantioselective recognition toward the Chiralcel OJ-H stationary phase.

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All Publications

2012: Simone Carradori; Roberto Cirilli; Simona Dei Cicchi; Rosella Ferretti; Sergio Menta; Marco Pierini; Daniela Secci
3-methylcyclohexanone thiosemicarbazone: determination of E/Z isomerization barrier by dynamic high-performance liquid chromatography, configuration assignment and theoretical study of the mechanisms involved by the spontaneous, acid and base catalyzed processes.
Journal of chromatography. A 2012;1269():168-77.
2012: dante rotili; Alberta Samuele; Domenico Tarantino; Ludovica Morera; Ira Musmuca; Maxim B Nawrozkij; Marco Pierini; Rino Ragno; Marino Artico; FLAVIO BALLANTE; Giorgia Botta; Roberto Cirilli; Bonaventura Clotet; José A Esté; Emmanuel Gonzalez; giovanni maga; Antonello Mai
2-(Alkyl/aryl)amino-6-benzylpyrimidin-4(3H)-ones as inhibitors of wild-type and mutant HIV-1: enantioselectivity studies.
Journal of medicinal chemistry 2012;55(7):3558-62.
2012: Stefano Alcaro; Adriana Bolasco; Roberto Cirilli; Rosella Ferretti; Rossella Fioravanti; Francesco Ortuso
Computer-aided molecular design of asymmetric pyrazole derivatives with exceptional enantioselective recognition toward the Chiralcel OJ-H stationary phase.
Journal of chemical information and modeling 2012;52(3):649-54.
2012: Daniela De Vita; Barbara Di Rienzo; Roberto Di Santo; Paolo Mellini; Simona Panella; Luigi Scipione; Giovanna Simonetti; Silvano Tortorella; Roberto Cirilli; Felicia Diodata D'Auria; Anna Teresa Palamara
Synthesis and antifungal activity of a new series of 2-(1H-imidazol-1-yl)-1-phenylethanol derivatives.
European journal of medicinal chemistry 2012;49():334-42.
2011: Rosella Ferretti; Bruno Gallinella; Antonello Mai; Sergio Valente; Leo Zanitti; Roberto Cirilli
Application of 3 μm particle-based amylose-derived chiral stationary phases for the enantioseparation of potential histone deacetylase inhibitors.
Journal of chromatography. A 2011;1218(46):8394-8.
2011: Elias Maccioni; Peter Matyus; Rita Meleddu; Maria Luisa Sanna; Sara Vigo; Matilde Yanez; Stefano Alcaro; Maria Cristina Cardia; Laura Casu; Roberto Cirilli; Giosuè Costa; Simona Distinto
3-Acetyl-2,5-diaryl-2,3-dihydro-1,3,4-oxadiazoles: a new scaffold for the selective inhibition of monoamine oxidase B.
Journal of medicinal chemistry 2011;54(18):6394-8.
2011: Gianluca Sbardella; Ilaria Sciamanna; Annalucia Serafino; Sara Bartolini; Sabrina Castellano; Roberto Cirilli; Patrizia Lavia; Antonello Mai; Ciro Milite; Serena Orlando; dante rotili; Marisabella Santoriello; Corrado Spadafora
Modulation of cell differentiation, proliferation, and tumor growth by dihydrobenzyloxopyrimidine non-nucleoside reverse transcriptase inhibitors.
Journal of medicinal chemistry 2011;54(16):5927-36.
2011: Roberto Cirilli; Stefano Alcaro; Adriana Bolasco; Rosella Ferretti; Rossella Fioravanti; Bruno Gallinella; Cristina Faggi
A chromatographic study on the exceptional enantioselectivity of cellulose tris(4-methylbenzoate) towards C5-chiral 4,5-dihydro-(1H)-pyrazole derivatives.
Journal of chromatography. A 2011;1218(33):5653-7.
2011: Sergio Valente; Maria Tardugno; Mariarosaria Conte; Roberto Cirilli; Andrea Perrone; Rino Ragno; Silvia Simeoni; Anna Tramontano; Silvio Massa; Angela Nebbioso; Marco Miceli; Gianluigi Franci; Gerald Brosch; Lucia Altucci; Antonello Mai
Novel cinnamyl hydroxyamides and 2-aminoanilides as histone deacetylase inhibitors: apoptotic induction and cytodifferentiation activity.
ChemMedChem 2011;6(4):698-712.
2010: Rossella Fioravanti; Adriana Bolasco; Fedele Manna; Francesca Rossi; Matilde Yañez; Francesco Ortuso; Stefano Alcaro; Roberto Cirilli
Synthesis and biological evaluation of N-substituted-3,5-diphenyl-2-pyrazoline derivatives as cyclooxygenase (COX-2) inhibitors.
European journal of medicinal chemistry 2010;45(12):6135-8.
2010: Roberto Cirilli; Rosella Ferretti; Giuseppe La Regina; Gianluigi Morelli; Marco Pierini; Francesco Piscitelli; Romano Silvestri
Enantioselective HPLC combined with spectroscopic methods: a valid strategy to determine the absolute configuration of potential beta-secretase inhibitors.
Talanta 2010;82(4):1306-12.
2010: Franco Chimenti; Daniela Secci; Adriana Bolasco; Paola Chimenti; Arianna Granese; Simone Carradori; Matilde Yáñez; Matilde Yañez; M Luisa Sanna; Bruno Gallinella; Roberto Cirilli
Synthesis, stereochemical separation, and biological evaluation of selective inhibitors of human MAO-B: 1-(4-arylthiazol-2-yl)-2-(3-methylcyclohexylidene)hydrazines.
Journal of medicinal chemistry 2010;53(17):6516-20.
2010: Leo Zanitti; Rosella Ferretti; Bruno Gallinella; Francesco La Torre; Maria Luisa Sanna; Antonina Mosca; Roberto Cirilli
Direct HPLC enantioseparation of omeprazole and its chiral impurities: application to the determination of enantiomeric purity of esomeprazole magnesium trihydrate.
Journal of pharmaceutical and biomedical analysis 2010;52(5):665-71.
2010: Franco Chimenti; Daniela Secci; Adriana Bolasco; Paola Chimenti; Arianna Granese; Simone Carradori; Elias Maccioni; M Cristina Cardia; Matilde Yáñez; Matilde Yañez; Stefano Alcaro; Francesco Ortuso; Roberto Cirilli; Rosella Ferretti; Simona Distinto; Johannes Kirchmair; Thierry Langer
Synthesis, semipreparative HPLC separation, biological evaluation, and 3D-QSAR of hydrazothiazole derivatives as human monoamine oxidase B inhibitors.
Bioorganic & medicinal chemistry 2010;18(14):5063-70.
2010: Maria Luisa Sanna; Elias Maccioni; Sara Vigo; Cristina Faggi; Roberto Cirilli
Application of an immobilised amylose-based chiral stationary phase to the development of new monoamine oxidase B inhibitors.
Talanta 2010;82(1):426-31.
2010: Franco Chimenti; Rossella Fioravanti; Adriana Bolasco; Paola Chimenti; Daniela Secci; Francesca Rossi; Matilde Yáñez; Matilde Yañez; Francesco Ortuso; Stefano Alcaro; Roberto Cirilli; Rosella Ferretti; M Luisa Sanna
A new series of flavones, thioflavones, and flavanones as selective monoamine oxidase-B inhibitors.
Bioorganic & medicinal chemistry 2010;18(3):1273-9.
2010: Serena Scapecchi; Marta Nesi; Rosanna Matucci; Cristina Bellucci; Michela Buccioni; Silvia Dei; Luca Guandalini; Dina Manetti; Cecilia Martelli; Elisabetta Martini; Gabriella Marucci; Francesca Orlandi; Maria Novella Romanelli; Elisabetta Teodori; Roberto Cirilli
Synthesis, affinity profile and functional activity of potent chiral muscarinic antagonists with a pyrrolidinylfuran structure.
Journal of medicinal chemistry 2010;53(1):201-7.
2010: Roberto Cirilli; Stefano Fiore; Francesco La Torre; Elias Maccioni; Daniela Secci; Maria Luisa Sanna; Cristina Faggi
Semipreparative HPLC enantioseparation, chiroptical properties, and absolute configuration of two novel cyclooxygenase-2 inhibitors.
Chirality 2010;22(1):56-62.
2009: Roberto Cirilli; Rosella Ferretti; Bruno Gallinella; Luciana Turchetto; Leo Zanitti; Francesco La Torre
Development and validation of an enantioselective and chemoselective HPLC method using a Chiralpak IA column to simultaneously quantify (R)-(+)- and (S)-(-)-lansoprazole enantiomers and related impurities.
Journal of pharmaceutical and biomedical analysis 2009;50(1):9-14.
2009: Rosella Ferretti; Bruno Gallinella; Francesco La Torre; Leo Zanitti; Luciana Turchetto; Antonina Mosca; Roberto Cirilli
Direct high-performance liquid chromatography enantioseparation of terazosin on an immobilised polysaccharide-based chiral stationary phase under polar organic and reversed-phase conditions.
Journal of chromatography. A 2009;1216(28):5385-90.
2009: Roberto Cirilli; Rosella Ferretti; Francesco La Torre; Anna Borioni; Vincenzo Fares; Mercedes Camalli; Cristina Faggi; Dante Rotili; Antonello Mai
Chiral HPLC separation and absolute configuration of novel S-DABO derivatives.
Chirality 2009;21(6):604-12.
2009: Roberto Cirilli; Stefano Alcaro; Rossella Fioravanti; Daniela Secci; Stefano Fiore; Francesco La Torre; Francesco Ortuso
Unusually high enantioselectivity in high-performance liquid chromatography using cellulose tris(4-methylbenzoate) as a chiral stationary phase.
Journal of chromatography. A 2009;1216(22):4673-8.
2009: Roberto Cirilli; Roberta Costi; Roberto Di Santo; Francesco La Torre; Marco Pierini; Gabriella Siani
Perturbing effects of chiral stationary phase on enantiomerization second-order rate constants determined by enantioselective dynamic high-performance liquid chromatography: a practical tool to quantify the accessible acid and basic catalytic sites bonded on chromatographic supports.
Analytical chemistry 2009;81(9):3560-70.
2009: Simona Rapposelli; Vincenzo Calderone; Roberto Cirilli; Maria Digiacomo; Cristina Faggi; Francesco La Torre; Mariaelisa Manganaro; Alma Martelli; Lara Testai
Enantioselectivity in cardioprotection induced by (S)- (-)-2,2-dimethyl-N-(4'-acetamido-benzyl)-4-spiromorpholone-chromane.
Journal of medicinal chemistry 2009;52(5):1477-80.
2009: Roberto Cirilli; Roberta Costi; Roberto Di Santo; Francesco Gasparrini; Francesco La Torre; Marco Pierini; Gabriella Siani
A rational approach to predict and modulate stereolability of chiral alpha substituted ketones.
Chirality 2009;21(1):24-34.
2008: Mariangela Biava; Giulio C Porretta; Giovanna Poce; Sibilla Supino; Fabrizio Manetti; Stefano Forli; Maurizio Botta; Lidia Sautebin; Antonietta Rossi; Carlo Pergola; Carla Ghelardini; Monica Norcini; Francesco Makovec; Antonio Giordani; Paola Anzellotti; Roberto Cirilli; Rosella Ferretti; Bruno Gallinella; Francesco La Torre; Maurizio Anzini; Paola Patrignani
Synthesis, in vitro, and in vivo biological evaluation and molecular docking simulations of chiral alcohol and ether derivatives of the 1,5-diarylpyrrole scaffold as novel anti-inflammatory and analgesic agents.
Bioorganic & medicinal chemistry 2008;16(17):8072-81.
2008: Franco Chimenti; Elias Maccioni; Daniela Secci; Adriana Bolasco; Paola Chimenti; Arianna Granese; Simone Carradori; Stefano Alcaro; Francesco Ortuso; Matilde Yáñez; Matilde Yañez; Roberto Cirilli; Rosella Ferretti; Francesco La Torre
Synthesis, stereochemical identification, and selective inhibitory activity against human monoamine oxidase-B of 2-methylcyclohexylidene-(4-arylthiazol-2-yl)hydrazones.
Journal of medicinal chemistry 2008;51(16):4874-80.
2008: Serena Scapecchi; Marta Nesi; Rosanna Matucci; Cristina Bellucci; Michela Buccioni; Silvia Dei; Luca Guandalini; Dina Manetti; Elisabetta Martini; Gabriella Marucci; Maria Novella Romanelli; Elisabetta Teodori; Roberto Cirilli
Synthesis and pharmacological characterization of chiral pyrrolidinylfuran derivatives: the discovery of new functionally selective muscarinic agonists.
Journal of medicinal chemistry 2008;51(13):3905-12.
2008: Giuseppe La Regina; Felicia Diodata D'Auria; Andrea Tafi; Francesco Piscitelli; Stefania Olla; Fabiana Caporuscio; Nencioni Lucia; Roberto Cirilli; Francesco La Torre; Nadja Rodrigues De Melo; Steven L Kelly; David C Lamb; Marino Artico; Maurizio Botta; Anna Teresa Palamara; Romano Silvestri
1-[(3-Aryloxy-3-aryl)propyl]-1H-imidazoles, new imidazoles with potent activity against Candida albicans and dermatophytes. Synthesis, structure-activity relationship, and molecular modeling studies.
Journal of medicinal chemistry 2008;51(13):3841-55.
2008: Roberto Cirilli; Rosella Ferretti; Bruno Gallinella; Anna Rita Bilia; Franco Francesco Vincieri; Francesco La Torre
Enantioseparation of kavain on Chiralpak IA under normal-phase, polar organic and reversed-phase conditions.
Journal of separation science 2008;31(12):2206-10.
2008: Mariangela Biava; Roberto Cirilli; Vincenzo Fares; Rosella Ferretti; Bruno Gallinella; Francesco La Torre; Giovanna Poce; Giulio Cesare Porretta; Sibilla Supino; Claudio Villani
HPLC enantioseparation and absolute configuration of novel anti-inflammatory pyrrole derivatives.
Chirality 2008;20(6):775-80.
2008: Roberto Cirilli; Rosella Ferretti; Emiliana De Santis; Bruno Gallinella; Leo Zanitti; Francesco La Torre
High-performance liquid chromatography separation of enantiomers of flavanone and 2'-hydroxychalcone under reversed-phase conditions.
Journal of chromatography. A 2008;1190(1-2):95-101.
2008: Svend B Jensen; Roberto Di Santo; Aage Kristian Olsen; Kasper Pedersen; Roberta Costi; Roberto Cirilli; Paul Cumming
Synthesis and cerebral uptake of 1-(1-[(11)C]methyl-1H-pyrrol-2-yl)-2-phenyl-2-(1-pyrrolidinyl)ethanone, a novel tracer for positron emission tomography studies of monoamine oxidase type A.
Journal of medicinal chemistry 2008;51(6):1617-22.
2008: Roberto Cirilli; Rosella Ferretti; Bruno Gallinella; Emiliana De Santis; Leo Zanitti; Francesco La Torre
High-performance liquid chromatography enantioseparation of proton pump inhibitors using the immobilized amylose-based Chiralpak IA chiral stationary phase in normal-phase, polar organic and reversed-phase conditions.
Journal of chromatography. A 2008;1177(1):105-13.
2007: Roberto Cirilli; Rosella Ferretti; Francesco La Torre; Daniela Secci; Adriana Bolasco; Simone Carradori; M Pierini
High-performance liquid chromatographic separation of enantiomers and diastereomers of 2-methylcyclohexanone thiosemicarbazone, and determination of absolute configuration and configurational stability.
Journal of chromatography. A 2007;1172(2):160-9.
2006: Romano Silvestri; Gabriella Marfè; Marino Artico; Giuseppe La Regina; Antonio Lavecchia; Ettore Novellino; Emanuela Morgante; Manuela Morgante; Carla Di Stefano; Gianfranco Catalano; Giuseppe Filomeni; Elisabetta Abruzzese; Maria Rosa Ciriolo; Matteo A Russo; Sergio Amadori; Roberto Cirilli; Francesco La Torre; Paola Sinibaldi-Salimei
Pyrrolo[1,2-b][1,2,5]benzothiadiazepines (PBTDs): A new class of agents with high apoptotic activity in chronic myelogenous leukemia K562 cells and in cells from patients at onset and who were imatinib-resistant.
Journal of medicinal chemistry 2006;49(19):5840-4.
2006: Roberto Cirilli; Viviana Orlando; Rosella Ferretti; Luciana Turchetto; Romano Silvestri; Gabriella De Martino; Francesco La Torre
Direct HPLC enantioseparation of chiral aptazepine derivatives on coated and immobilized polysaccharide-based chiral stationary phases.
Chirality 2006;18(8):621-32.
2006: Roberto Cirilli; Rosella Ferretti; Bruno Gallinella; Francesco La Torre; Antonello Mai; Dante Rotili
Analytical and semipreparative high performance liquid chromatography separation of stereoisomers of novel 3,4-dihydropyrimidin-4(3H)-one derivatives on the immobilised amylose-based Chiralpak IA chiral stationary phase.
Journal of separation science 2006;29(10):1399-406.
2006: Roberto Cirilli; A Simonelli; Rosella Ferretti; Adriana Bolasco; Paola Chimenti; Daniela Secci; Elias Maccioni; Francesco La Torre
Analytical and semipreparative high performance liquid chromatography enantioseparation of new substituted 1-thiocarbamoyl-3,5-diaryl-4,5-dihydro-(1H)-pyrazoles on polysaccharide-based chiral stationary phases in normal-phase, polar organic and reversed-phase conditions.
Journal of chromatography. A 2006;1101(1-2):198-203.
2006: Roberto Di Santo; Roberta Costi; Marino Artico; Rino Ragno; Antonio Lavecchia; Ettore Novellino; Enrico Gavuzzo; Francesco La Torre; Roberto Cirilli; Reynel Cancio; giovanni maga
Design, synthesis, biological evaluation, and molecular modeling studies of TIBO-like cyclic sulfones as non-nucleoside HIV-1 reverse transcriptase inhibitors.
ChemMedChem 2006;1(1):82-95.
2006: Franco Chimenti; Adriana Bolasco; Fedele Manna; Daniela Secci; Paola Chimenti; Arianna Granese; Olivia Befani; Paola Turini; Roberto Cirilli; Francesco La Torre; Stefano Alcaro; Francesco Ortuso; Thierry Langer
Synthesis, biological evaluation and 3D-QSAR of 1,3,5-trisubstituted-4,5-dihydro-(1H)-pyrazole derivatives as potent and highly selective monoamine oxidase A inhibitors.
Current medicinal chemistry 2006;13(12):1411-28.
2005: Franco Chimenti; Elias Maccioni; Daniela Secci; Adriana Bolasco; Paola Chimenti; Arianna Granese; Olivia Befani; Paola Turini; Stefano Alcaro; Francesco Ortuso; Roberto Cirilli; Francesco La Torre; Maria C Cardia; Simona Distinto
Synthesis, molecular modeling studies, and selective inhibitory activity against monoamine oxidase of 1-thiocarbamoyl-3,5-diaryl-4,5-dihydro-(1H)- pyrazole derivatives.
Journal of medicinal chemistry 2005;48(23):7113-22.
2005: Gabriella De Martino; Giuseppe La Regina; Francesco La Torre; Roberto Cirilli; Ilario Mereghetti; Alfredo Cagnotto; Marino Artico; Romano Silvestri
Chiral resolution and binding study of 1,3,4,14b-tetrahydro-2,10-dimethyl-2H,10H-pyrazino[2,1-d]pyrrolo[1,2-b] [1,2,5]benzotriazepine (10-methyl-10-azaaptazepine) and 2-methyl-1,3,4,14b-tetrahydro-2H-pyrazino[2,1-d]pyrrolo[1,2-b] [1,2,5]benzothiadiazepine 10,10-dioxide (tiaaptazepine).
Farmaco (Società chimica italiana : 1989) 2005;60(11-12):931-7.
2005: Roberto Di Santo; Roberta Costi; Alessandra Roux; Marino Artico; Olivia Befani; Tiziana Meninno; Enzo Agostinelli; Paola Palmegiani; Paola Turini; Roberto Cirilli; Rosella Ferretti; Bruno Gallinella; Francesco La Torre
Design, synthesis, and biological activities of pyrrolylethanoneamine derivatives, a novel class of monoamine oxidases inhibitors.
Journal of medicinal chemistry 2005;48(13):4220-3.
2005: Roberto Cirilli; Rosella Ferretti; Bruno Gallinella; Francesco La Torre; Giuseppe La Regina; Romano Silvestri
Comparative study between the polysaccharide-based chiralcel OJ and chiralcel OD CSPSs in chromatographic enantioseparation of imidazole analogues of fluoxetine and miconazole.
Journal of separation science 2005;28(7):627-34.
2004: Roberto Cirilli; Rosella Ferretti; Bruno Gallinella; Leo Zanitti; Francesco La Torre
A new application of stopped-flow chiral HPLC: inversion of enantiomer elution order.
Journal of chromatography. A 2004;1061(1):27-34.
2004: Roberto Cirilli; Rosella Ferretti; Bruno Gallinella; Luciana Turchetto; Adriana Bolasco; Daniela Secci; Paola Chimenti; Marco Pierini; Vincenzo Fares; Olivia Befani; Francesco La Torre
Enantiomers of C(5)-chiral 1-acetyl-3,5-diphenyl-4,5-dihydro-(1H)-pyrazole derivatives: Analytical and semipreparative HPLC separation, chiroptical properties, absolute configuration, and inhibitory activity against monoamine oxidase.
Chirality 2004;16(9):625-36.
2004: Franco Chimenti; Adriana Bolasco; Fedele Manna; Daniela Secci; Paola Chimenti; Olivia Befani; Paola Turini; Valentina Giovannini; Bruno Mondovì; Roberto Cirilli; Francesco La Torre
Synthesis and selective inhibitory activity of 1-acetyl-3,5-diphenyl-4,5-dihydro-(1H)-pyrazole derivatives against monoamine oxidase.
Journal of medicinal chemistry 2004;47(8):2071-4.
2003: Francesco La Torre; Roberto Cirilli; Rosella Ferretti; Bruno Gallinella; Roberta Costi; Roberto Di Santo
Conversion of a racemic mixture of 8-chloro-2-(2,6-difluorophenylmethyl)-2,3-dihydro-3-methyl-1,2,5-benzothiadiazepin-4(5h)-one 1,1-dioxide into a single enantiomer via a chromatographic resolution/racemization method.
Chirality 2003;15(5):429-32.
2003: Roberto Cirilli; Roberta Costi; Roberto Di Santo; Marino Artico; Alessandra Roux; Bruno Gallinella; Leo Zanitti; Francesco La Torre
Enantioselective liquid chromatography of C3-chiral 2,3-dihydro-1,2,5-benzothiadiazepin-4(5H)-one and thione 1,1-dioxides on polyacrylamide- and polysaccharide-based chiral stationary phases.
Journal of chromatography. A 2003;993(1-2):17-28.
2002: Roberto Cirilli; Roberta Costi; Santo R Di; Rosella Ferretti; Torre F La; Letizia Angiolella; M Micocci
Analytical and semipreparative enantiomeric separation of azole antifungal agents by high-performance liquid chromatography on polysaccharide-based chiral stationary phases. Application to in vitro biological studies.
Journal of chromatography. A 2002;942(1-2):107-14.
2001: Roberto Cirilli; Maria Rosaria Del Giudice; Rosella Ferretti; Francesco La Torre
Conformational and temperature effects on separation of stereoisomers of a C3,C4-substituted beta-lactamic cholesterol absorption inhibitor on amylose-based chiral stationary phases.
Journal of chromatography. A 2001;923(1-2):27-36.