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Ph Hubert

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Iolanda Nistor; R Oprean; Ines Slama; Eduard Badarau; Attilio Ceccato; Katina Sourou Sylvestre Dossou; Fabien Dufour; Marianne Fillet; Ph Hubert; Pierre Lebrun; Frédéric Lecomte; Jean-François Liégeois; Eric Rozet
Implementation of a design space approach for enantiomeric separations in polar organic solvent chromatography.
J K Mbinze; Eric Rozet; T Schofield; J Mavar Tayey Mbay; B Boulanger; B Debrus; A Dispas; Ph Hubert; N Kalenda; P Lebrun; R D Marini
Application of an innovative design space optimization strategy to the development of liquid chromatographic methods to combat potentially counterfeit nonsteroidal anti-inflammatory drugs.
Eric Rozet; Eric Ziemons; Bruno Boulanger; Roland Djang'eing'a Marini; Ph Hubert
Validation of analytical methods involved in dissolution assays: acceptance limits and decision methodologies.

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2013: Iolanda Nistor; R Oprean; Ines Slama; Eduard Badarau; Attilio Ceccato; Katina Sourou Sylvestre Dossou; Fabien Dufour; Marianne Fillet; Ph Hubert; Pierre Lebrun; Frédéric Lecomte; Jean-François Liégeois; Eric Rozet
Implementation of a design space approach for enantiomeric separations in polar organic solvent chromatography.
Journal of pharmaceutical and biomedical analysis 2013;74():273-83.
2012: J K Mbinze; Eric Rozet; T Schofield; J Mavar Tayey Mbay; B Boulanger; B Debrus; A Dispas; Ph Hubert; N Kalenda; P Lebrun; R D Marini
Application of an innovative design space optimization strategy to the development of liquid chromatographic methods to combat potentially counterfeit nonsteroidal anti-inflammatory drugs.
Journal of chromatography. A 2012;1263():113-24.
2012: Eric Rozet; Eric Ziemons; Bruno Boulanger; Roland Djang'eing'a Marini; Ph Hubert
Validation of analytical methods involved in dissolution assays: acceptance limits and decision methodologies.
Analytica chimica acta 2012;751():44-51.
2012: A L S Dias; Ph Hubert; A C Oliveira; C A S Rabelo; H Rogez; Eric Rozet; G Chataigné; Joëlle Quetin-Leclercq
A rapid validated UHPLC-PDA method for anthocyanins quantification from Euterpe oleracea fruits.
Journal of chromatography. B, Analytical technologies in the biomedical and life sciences 2012;907():108-16.
2012: C De Bleye; Ph Hubert; J Mantanus; Roland Djang'eing'a Marini; Eric Rozet; P-F Chavez; Eric Ziemons
Critical review of near-infrared spectroscopic methods validations in pharmaceutical applications.
Journal of pharmaceutical and biomedical analysis 2012;69():125-32.
2012: Caroline Lamalle; Pierre Lebrun; Anne-Catherine Servais; Roland Djang'eing'a Marini; Jacques Crommen; Benjamin Debrus; Ph Hubert; Marianne Fillet
Development of a generic micellar electrokinetic chromatography method for the separation of 15 antimalarial drugs as a tool to detect medicine counterfeiting.
Electrophoresis 2012;33(11):1669-78.
2012: A Bouabidi; A Bouklouze; Bruno Boulanger; H Bourichi; C Hubert; Ph Hubert; Roland Djang'eing'a Marini; M Talbi; Eric Ziemons; M El Karbane; Eric Rozet
Usefulness of capability indices in the framework of analytical methods validation.
Analytica chimica acta 2012;714():47-56.
2012: Eric Rozet; Eric Ziemons; Bruno Boulanger; Roland Djang'eing'a Marini; Ph Hubert
Comments on "uncertainty profiles for the validation of analytical methods" by Saffaj and Ihssane.
Talanta 2012;88():769-71.
2012: Eric Rozet; Eric Ziemons; Bruno Boulanger; Roland Djang'eing'a Marini; Ph Hubert
Quality by design compliant analytical method validation.
Analytical chemistry 2012;84(1):106-12.
2011: Eric Rozet; Serge Rudaz; Reinhold Wintersteiger; Eric Ziemons; Bruno Boulanger; Bernadette Govaerts; Pierre Lebrun; Karim Michail; Ph Hubert
Evaluating the reliability of analytical results using a probability criterion: a Bayesian perspective.
Analytica chimica acta 2011;705(1-2):193-206.
2011: Eric Rozet; Serge Rudaz; E Ziémons; Bruno Boulanger; R D Marini; Ph Hubert
Models to estimate overall analytical measurements uncertainty: assumptions, comparisons and applications.
Analytica chimica acta 2011;702(2):160-71.
2011: I Nistor; R Oprean; Eric Rozet; P Lebrun; F Lecomte; L Angenot; M Cao; B Debrus; M Frederich; Ph Hubert
Application of a new optimization strategy for the separation of tertiary alkaloids extracted from Strychnos usambarensis leaves.
Journal of pharmaceutical and biomedical analysis 2011;56(1):30-7.
2011: J Mantanus; Eric Rozet; K Van Butsele; Attilio Ceccato; C De Bleye; Brigitte Evrard; Ph Hubert; E Ziémons
Near infrared and Raman spectroscopy as Process Analytical Technology tools for the manufacturing of silicone-based drug reservoirs.
Analytica chimica acta 2011;699(1):96-106.
2011: E Ziémons; H Bourichi; J Mantanus; Eric Rozet; P Lebrun; E Essassi; Y Cherrah; A Bouklouze; Ph Hubert
Determination of binary polymorphic mixtures of fluconazole using near infrared spectroscopy and X-ray powder diffraction: a comparative study based on the pre-validation stage results.
Journal of pharmaceutical and biomedical analysis 2011;55(5):1208-12.
2011: Eric Rozet; Roland Djang'eing'a Marini; Eric Ziemons; Bruno Boulanger; Ph Hubert
Advances in validation, risk and uncertainty assessment of bioanalytical methods.
Journal of pharmaceutical and biomedical analysis 2011;55(4):848-58.
2011: A Gillet; P Compère; F Lecomte; Ph Hubert; E Ducat; Brigitte Evrard; Géraldine Piel
Liposome surface charge influence on skin penetration behaviour.
International journal of pharmaceutics 2011;411(1-2):223-31.
2011: A Bouabidi; M Talbi; A Bouklouze; M El Karbane; H Bourichi; M El Guezzar; Eric Ziemons; Ph Hubert; Eric Rozet
Do placebo based validation standards mimic real batch products behaviour? Case studies.
Journal of pharmaceutical and biomedical analysis 2011;55(3):583-90.
2011: Fabrice Krier; Michaël Brion; Benjamin Debrus; Pierre Lebrun; Aurélie Driesen; Eric Ziemons; Brigitte Evrard; Ph Hubert
Optimisation and validation of a fast HPLC method for the quantification of sulindac and its related impurities.
Journal of pharmaceutical and biomedical analysis 2011;54(4):694-700.
2010: Jérôme Mantanus; Eric Ziémons; Eric Rozet; Bruno Streel; Régis Klinkenberg; Brigitte Evrard; Jukka Rantanen; Ph Hubert
Building the quality into pellet manufacturing environment--feasibility study and validation of an in-line quantitative near infrared (NIR) method.
Talanta 2010;83(2):305-11.
2010: E Ziémons; J Mantanus; P Lebrun; Eric Rozet; Brigitte Evrard; Ph Hubert
Acetaminophen determination in low-dose pharmaceutical syrup by NIR spectroscopy.
Journal of pharmaceutical and biomedical analysis 2010;53(3):510-6.
2010: Etienne Cavalier; Eric Rozet; R Gadisseur; Agnès Carlisi; M Monge; Jean-Paul Chapelle; Ph Hubert; Jean-Claude Souberbielle; Pierre Delanaye
Measurement uncertainty of 25-OH vitamin D determination with different commercially available kits: impact on the clinical cut offs.
Osteoporosis international : a journal established as result of cooperation between the European Foundation for Osteoporosis and the National Osteoporosis Foundation of the USA 2010;21(6):1047-51.
2010: J Mantanus; E Ziémons; Philippe Lebrun; Eric Rozet; R Klinkenberg; Bruno Streel; B Evrard; Ph Hubert
Active content determination of non-coated pharmaceutical pellets by near infrared spectroscopy: method development, validation and reliability evaluation.
Talanta 2010;80(5):1750-7.
2010: Edith Staes; Eric Rozet; Bernard Ucakar; Ph Hubert; Véronique Préat
Validation of a method for the quantitation of ghrelin and unacylated ghrelin by HPLC.
Journal of pharmaceutical and biomedical analysis 2010;51(3):633-9.
2010: C Hubert; E Ziémons; Eric Rozet; A Breuer; A Lambert; C Jasselette; C De Bleye; Robert G Lejeune; Ph Hubert
Development and validation of a quantitative method for the selective determination of tin species in tin octoate by differential pulse polarography.
Talanta 2010;80(3):1413-20.
2010: Etienne Cavalier; Eric Rozet; Agnès Carlisi; Anne-Catherine Bekaert; Olivier Rousselle; Ph Hubert; Jean-Paul Chapelle; Pierre Delanaye
Analytical validation of serum bone alkaline phosphatase (BAP OSTASE) on Liaison.
Clinical chemistry and laboratory medicine : CCLM / FESCC 2010;48(1):67-72.
2009: Benjamin De Backer; Benjamin Debrus; Pierre Lebrun; Laetitia Theunis; Nathalie Dubois; Lies Decock; Alain Verstraete; Ph Hubert; Corinne Charlier
Innovative development and validation of an HPLC/DAD method for the qualitative and quantitative determination of major cannabinoids in cannabis plant material.
Journal of chromatography. B, Analytical technologies in the biomedical and life sciences 2009;877(32):4115-24.
2009: Gaëlle B Martin; François Mansion; Anne-Catherine Servais; Benjamin Debrus; Eric Rozet; Ph Hubert; Jacques Crommen; Marianne Fillet
CE-MS method development for peptides analysis, especially hepcidin, an iron metabolism marker.
Electrophoresis 2009;30(15):2624-31.
2009: François Boemer; Vincent Bours; Roland Schoos; Ph Hubert; Eric Rozet
Analytical validation based on total error measurement and cut-off interpretation of a neonatal screening TSH-immunoassay.
Journal of chromatography. B, Analytical technologies in the biomedical and life sciences 2009;877(23):2412-7.
2009: Benjamin Debrus; Pierre Lebrun; Attilio Ceccato; Gabriel Caliaro; Bernadette Govaerts; Bernard A Olsen; Eric Rozet; Bruno Boulanger; Ph Hubert
A new statistical method for the automated detection of peaks in UV-DAD chromatograms of a sample mixture.
Talanta 2009;79(1):77-85.
2009: J Mantanus; E Ziémons; Philippe Lebrun; Eric Rozet; R Klinkenberg; Bruno Streel; B Evrard; Ph Hubert
Moisture content determination of pharmaceutical pellets by near infrared spectroscopy: method development and validation.
Analytica chimica acta 2009;642(1-2):186-92.
2008: Ph Hubert; JJ Nguyen-Huu; Bruno Boulanger; E Chapuzet; N Cohen; PA Compagnon; Walthère Dewé; Max Feinberg; M Laurentie; N Mercier; G Muzard; L Valat; Eric Rozet
Harmonization of strategies for the validation of quantitative analytical procedures: a SFSTP proposal part IV. Examples of application.
Journal of pharmaceutical and biomedical analysis 2008;48(3):760-71.
2008: Etienne Cavalier; Eric Rozet; Nathalie Dubois; Corinne Charlier; Ph Hubert; Jean-Paul Chapelle; Jean-Marie Krzesinski; Pierre Delanaye
Performance of iohexol determination in serum and urine by HPLC: validation, risk and uncertainty assessment.
Clinica chimica acta; international journal of clinical chemistry 2008;396(1-2):80-5.
2008: Valentine Wascotte; Eric Rozet; Ana Salvaterra; Ph Hubert; Michel Jadoul; Richard H Guy; Véronique Préat
Non-invasive diagnosis and monitoring of chronic kidney disease by reverse iontophoresis of urea in vivo.
European journal of pharmaceutics and biopharmaceutics : official journal of Arbeitsgemeinschaft für Pharmazeutische Verfahrenstechnik e.V 2008;69(3):1077-82.
2008: Eric Rozet; Walthère Dewé; R Morello; Patrice Chiap; F Lecomte; Eric Ziemons; KS Boos; Bruno Boulanger; Jacques Crommen; Ph Hubert
Risk-based approach for the transfer of quantitative methods: bioanalytical applications.
Journal of chromatography. A 2008;1189(1-2):32-41.
2008: M A Bimazubute; Eric Rozet; Isabelle Dizier; P Gustin; Ph Hubert; Jacques Crommen; Patrice Chiap
Liquid chromatographic determination of enrofloxacin in nasal secretions and plasma of healthy pigs using restricted access material for on-line sample clean-up.
Journal of chromatography. A 2008;1189(1-2):456-66.
2007: C Bodson; Eric Rozet; Eric Ziemons; Brigitte Evrard; Ph Hubert; Luc Delattre
Validation of manufacturing process of Diltiazem HCl tablets by NIR spectrophotometry (NIRS).
Journal of pharmaceutical and biomedical analysis 2007;45(2):356-61.
2007: Ph Hubert; JJ Nguyen-Huu; Bruno Boulanger; E Chapuzet; N Cohen; PA Compagnon; Walthère Dewé; Max Feinberg; M Laurentie; N Mercier; G Muzard; L Valat; Eric Rozet
Harmonization of strategies for the validation of quantitative analytical procedures. A SFSTP proposal--part III.
Journal of pharmaceutical and biomedical analysis 2007;45(1):82-96.
2007: Ph Hubert; JJ Nguyen-Huu; Bruno Boulanger; E Chapuzet; Patrice Chiap; N Cohen; PA Compagnon; Walthère Dewé; Max Feinberg; M Lallier; M Laurentie; N Mercier; G Muzard; C Nivet; L Valat; Eric Rozet
Harmonization of strategies for the validation of quantitative analytical procedures. A SFSTP proposal--part II.
Journal of pharmaceutical and biomedical analysis 2007;45(1):70-81.
2007: Eric Rozet; Attilio Ceccato; Cédric Hubert; Eric Ziemons; Radu Oprean; Serge Rudaz; Bruno Boulanger; Ph Hubert
Analysis of recent pharmaceutical regulatory documents on analytical method validation.
Journal of chromatography. A 2007;1158(1-2):111-25.
2007: Eric Rozet; Cédric Hubert; Attilio Ceccato; Walthère Dewé; Eric Ziemons; François Moonen; Karim Michail; Reinhold Wintersteiger; Bruno Streel; Bruno Boulanger; Ph Hubert
Using tolerance intervals in pre-study validation of analytical methods to predict in-study results. The fit-for-future-purpose concept.
Journal of chromatography. A 2007;1158(1-2):126-37.
2007: Roland Djang'eing'a Marini; Eric Rozet; Yvan Vander Heyden; Eric Ziemons; Bruno Boulanger; A Bouklouze; Anne-Catherine Servais; Marianne Fillet; Jacques Crommen; Ph Hubert
Robustness testing of a chiral NACE method for R-timolol determination in S-timolol maleate and uncertainty assessment from quantitative data.
Journal of pharmaceutical and biomedical analysis 2007;44(3):640-51.
2007: Gaëlle B Martin; Patrice Chiap; Philippe Paquet; Gerald E Pierard; Pascal de Tullio; Yves Martin; Eric Rozet; Ph Hubert; Jacques Crommen; Marianne Fillet
Development of a mass spectrometry method for the determination of a melanoma biomarker, 5-S-cysteinyldopa, in human plasma using solid phase extraction for sample clean-up.
Journal of chromatography. A 2007;1156(1-2):141-8.
2007: Valentine Wascotte; M Begoña Delgado-Charro; Eric Rozet; Pierre Wallemacq; Ph Hubert; Richard H Guy; Véronique Préat
Monitoring of urea and potassium by reverse iontophoresis in vitro.
Pharmaceutical research 2007;24(6):1131-7.
2007: Eric Rozet; Valentine Wascotte; N Lecouturier; Véronique Préat; Walthère Dewé; Bruno Boulanger; Ph Hubert
Improvement of the decision efficiency of the accuracy profile by means of a desirability function for analytical methods validation. Application to a diacetyl-monoxime colorimetric assay used for the determination of urea in transdermal iontophoretic extracts.
Analytica chimica acta 2007;591(2):239-47.
2007: E Ziémons; Georges Dive; B Debrus; Valéry Barillaro; Michel Frederich; Robert G Lejeune; Luc Angenot; Luc Delattre; L Thunus; Ph Hubert
Study of the physicochemical properties in aqueous medium and molecular modeling of tagitinin C/cyclodextrin complexes.
Journal of pharmaceutical and biomedical analysis 2007;43(3):910-9.
2006: Eric Rozet; R Morello; F Lecomte; G B Martin; Patrice Chiap; Jacques Crommen; KS Boos; Ph Hubert
Performances of a multidimensional on-line SPE-LC-ECD method for the determination of three major catecholamines in native human urine: validation, risk and uncertainty assessments.
Journal of chromatography. B, Analytical technologies in the biomedical and life sciences 2006;844(2):251-60.
2006: Eric Rozet; B Mertens; W Dewe; Attilio Ceccato; B Govaerts; Bruno Boulanger; Patrice Chiap; Bruno Streel; Jacques Crommen; Ph Hubert
The transfer of a LC-UV method for the determination of fenofibrate and fenofibric acid in Lidoses: use of total error as decision criterion.
Journal of pharmaceutical and biomedical analysis 2006;42(1):64-70.
2006: Roland Djang'eing'a Marini; Anne-Catherine Servais; Eric Rozet; Patrice Chiap; Bruno Boulanger; Serge Rudaz; Jacques Crommen; Ph Hubert; Marianne Fillet
Nonaqueous capillary electrophoresis method for the enantiomeric purity determination of S-timolol using heptakis(2,3-di-O-methyl-6-O-sulfo)-beta-cyclodextrin: validation using the accuracy profile strategy and estimation of uncertainty.
Journal of chromatography. A 2006;1120(1-2):102-11.
2006: C Bodson; Walthère Dewé; Ph Hubert; Luc Delattre
Comparison of FT-NIR transmission and UV-vis spectrophotometry to follow the mixing kinetics and to assay low-dose tablets containing riboflavin.
Journal of pharmaceutical and biomedical analysis 2006;41(3):783-90.
2006: Thao Do Thi; Romeo Pomponio; Roberto Gotti; Jan Saevels; Ben Van Hove; Willy Van Ael; Nele Matthijs; Yvan Vander Heyden; Roland Marini Djan'geing'a; Patrice Chiap; Ph Hubert; Jacques Crommen; Huguette Fabre; Pieter Dehouck; Jos Hoogmartens; Ann Van Schepdael
Precision study on capillary electrophoresis methods for metacycline.
Electrophoresis 2006;27(12):2317-29.
2006: Roland Djang'eing'a Marini; Carl Groom; François R Doucet; Jalal Hawari; Yaser Bitar; Ulrike Holzgrabe; Roberto Gotti; Julie Schappler; Serge Rudaz; Jean-Luc Veuthey; Roelof Mol; Govert W Somsen; Gerhardus J De Jong; Pham Thi Thanh Ha; Jie Zhang; Ann Van Schepdael; Jos Hoogmartens; Willy Briône; Attilio Ceccato; Bruno Boulanger; Debby Mangelings; Yvan Vander Heyden; Willy Van Ael; Ilias Jimidar; Matteo Pedrini; Anne-Catherine Servais; Marianne Fillet; Jacques Crommen; Eric Rozet; Ph Hubert
Interlaboratory study of a NACE method for the determination of R-timolol content in S-timolol maleate: assessment of uncertainty.
Electrophoresis 2006;27(12):2386-99.
2006: Virginie Esters; Luc Angenot; Viviane Brandt; Michel Frederich; Monique Tits; Christophe Van Nerum; Jean-Noël Wauters; Ph Hubert
Validation of a high-performance thin-layer chromatography/densitometry method for the quantitative determination of glucosamine in a herbal dietary supplement.
Journal of chromatography. A 2006;1112(1-2):156-64.
2006: Roland Djang'eing'a Marini; Patrice Chiap; Bruno Boulanger; Serge Rudaz; Eric Rozet; Jacques Crommen; Ph Hubert
LC method for the determination of R-timolol in S-timolol maleate: Validation of its ability to quantify and uncertainty assessment.
Talanta 2006;68(4):1166-75.
2006: Roland Djang'eing'a Marini; Patrice Chiap; Bruno Boulanger; Serge Rudaz; Eric Rozet; Jacques Crommen; Ph Hubert
[Comparison of three approaches for uncertainty estimation].
Acta clinica Belgica. Supplementum 2006;(1):60-2.
2006: Eric Rozet; Walthère Dewé; Patrice Chiap; F Lecomte; Ph Hubert
[The transfer of an automated method for the determination of noradrenaline in human urine: using total error as decision criterion].
Acta clinica Belgica. Supplementum 2006;(1):57-9.
2006: Ph Hubert; Eric Rozet; Bruno Boulanger; Walthère Dewé; M Laurentie; Nathalie Dubois; Corinne Charlier; Max Feinberg
[Harmonisation of validation strategies and estimation of the associated uncertainty in the framework of assay laboratoires accreditation].
Acta clinica Belgica. Supplementum 2006;(1):54-6.
2005: Anne-Catherine Servais; Marianne Fillet; Patrice Chiap; Walthère Dewé; Ph Hubert; Jacques Crommen
Influence of the nature of the electrolyte on the chiral separation of basic compounds in nonaqueous capillary electrophoresis using heptakis(2,3-di-O-methyl-6-O-sulfo)-beta-cyclodextrin.
Journal of chromatography. A 2005;1068(1):143-50.
2005: Patrice Chiap; Marie Piette; Brigitte Evrard; Francis Frankenne; B Christiaens; Géraldine Piel; Didier Cataldo; Jean-Michel Foidart; Luc Delattre; Jacques Crommen; Ph Hubert
Automated method for the determination of a new matrix metalloproteinase inhibitor in ovine plasma and serum by coupling of restricted access material for on-line sample clean-up to liquid chromatography.
Journal of chromatography. B, Analytical technologies in the biomedical and life sciences 2005;817(1):109-17.
2005: Bruno Streel; Attilio Ceccato; R Klinkenberg; Ph Hubert
Validation of a liquid chromatographic-tandem mass spectrometric method for the determination of loperamide in human plasma.
Journal of chromatography. B, Analytical technologies in the biomedical and life sciences 2005;814(2):263-73.
2005: O Rbeida; Patrice Chiap; Dieter Lubda; KS Boos; Jacques Crommen; Ph Hubert
Development and validation of a fully automated LC method for the determination of cloxacillin in human plasma using anion exchange restricted access material for sample clean-up.
Journal of pharmaceutical and biomedical analysis 2005;36(5):961-8.
2005: O Rbeida; B Christiaens; Ph Hubert; Dieter Lubda; KS Boos; Jacques Crommen; Patrice Chiap
Integrated on-line sample clean-up using cation exchange restricted access sorbent for the LC determination of atropine in human plasma coupled to UV detection.
Journal of pharmaceutical and biomedical analysis 2005;36(5):947-54.
2004: Ph Hubert; JJ Nguyen-Huu; Bruno Boulanger; E Chapuzet; Patrice Chiap; N Cohen; PA Compagnon; Walthère Dewé; Max Feinberg; M Lallier; M Laurentie; N Mercier; G Muzard; C Nivet; L Valat
Harmonization of strategies for the validation of quantitative analytical procedures. A SFSTP proposal--Part I.
Journal of pharmaceutical and biomedical analysis 2004;36(3):579-86.
2004: B Christiaens; Marianne Fillet; Patrice Chiap; O Rbeida; Attilio Ceccato; Bruno Streel; J De Graeve; Jacques Crommen; Ph Hubert
Fully automated method for the liquid chromatographic-tandem mass spectrometric determination of cyproterone acetate in human plasma using restricted access material for on-line sample clean-up.
Journal of chromatography. A 2004;1056(1-2):105-10.
2004: Max Feinberg; Bruno Boulanger; Walthère Dewé; Ph Hubert
New advances in method validation and measurement uncertainty aimed at improving the quality of chemical data.
Analytical and bioanalytical chemistry 2004;380(3):502-14.
2004: Sandrine Henry de Hassonville; Patrice Chiap; Jean-François Liégeois; Brigitte Evrard; Luc Delattre; Jacques Crommen; Géraldine Piel; Ph Hubert
Development and validation of a high-performance liquid chromatographic method for the determination of cyproterone acetate in human skin.
Journal of pharmaceutical and biomedical analysis 2004;36(1):133-43.
2004: Anne-Catherine Servais; Marianne Fillet; Patrice Chiap; Walthère Dewé; Ph Hubert; Jacques Crommen
Enantiomeric separation of basic compounds using heptakis(2,3-di-O-methyl-6-O-sulfo)-beta-cyclodextrin in combination with potassium camphorsulfonate in nonaqueous capillary electrophoresis: optimization by means of an experimental design.
Electrophoresis 2004;25(16):2701-10.
2004: Anne-Catherine Servais; Patrice Chiap; Ph Hubert; Jacques Crommen; Marianne Fillet
Determination of salbutamol enantiomers in human urine using heptakis(2,3-di-O-acetyl-6-O-sulfo)-beta-cyclodextrin in nonaqueous capillary electrophoresis.
Electrophoresis 2004;25(10-11):1632-40.
2004: O Rbeida; B Christiaens; Ph Hubert; Dieter Lubda; KS Boos; Jacques Crommen; Patrice Chiap
Evaluation of a novel anion-exchange restricted-access sorbent for on-line sample clean-up prior to the determination of acidic compounds in plasma by liquid chromatography.
Journal of chromatography. A 2004;1030(1-2):95-102.
2003: B Christiaens; Patrice Chiap; O Rbeida; D Cello; Jacques Crommen; Ph Hubert
Fully automated method for the liquid chromatographic determination of cyproterone acetate in plasma using restricted access material for sample pre-treatment.
Journal of chromatography. B, Analytical technologies in the biomedical and life sciences 2003;795(1):73-82.
2003: Pieter Dehouck; Yvan Vander Heyden; Johanna Smeyers-Verbeke; D Luc Massart; Roland Djang'eing'a Marini; Patrice Chiap; Ph Hubert; Jacques Crommen; W Van de Wauw; Jacques De Beer; R Cox; G Mathieu; J C Reepmeyer; B Voigt; O Estevenon; A Nicolas; Ann Van Schepdael; Erwin Adams; Jos Hoogmartens
Interlaboratory study of a liquid chromatography method for erythromycin: determination of uncertainty.
Journal of chromatography. A 2003;1010(1):63-74.
2003: O Rbeida; B Christiaens; Patrice Chiap; Ph Hubert; Dieter Lubda; KS Boos; Jacques Crommen
Fully automated LC method for the determination of sotalol in human plasma using restricted access material with cation exchange properties for sample clean-up.
Journal of pharmaceutical and biomedical analysis 2003;32(4-5):829-38.
2003: Bruno Boulanger; Patrice Chiap; W Dewe; Jacques Crommen; Ph Hubert
An analysis of the SFSTP guide on validation of chromatographic bioanalytical methods: progress and limitations.
Journal of pharmaceutical and biomedical analysis 2003;32(4-5):753-65.
2003: Attilio Ceccato; R Klinkenberg; Ph Hubert; Bruno Streel
Sensitive determination of buprenorphine and its N-dealkylated metabolite norbuprenorphine in human plasma by liquid chromatography coupled to tandem mass spectrometry.
Journal of pharmaceutical and biomedical analysis 2003;32(4-5):619-31.
2003: Roger Messin; Tamás Fenyvesi; Fabienne Carreer-Bruhwyler; Jacques Crommen; Patrice Chiap; Ph Hubert; Claude Dubois; Jean-Pierre Famaey; Joseph Géczy
A pilot double-blind randomized placebo-controlled study of molsidomine 16 mg once-a-day in patients suffering from stable angina pectoris: correlation between efficacy and over time plasma concentrations.
European journal of clinical pharmacology 2003;59(3):227-32.
2003: Anne-Catherine Servais; Marianne Fillet; Adel M Abushoffa; Ph Hubert; Jacques Crommen
Synergistic effects of ion-pairing in the enantiomeric separation of basic compounds with cyclodextrin derivatives in nonaqueous capillary electrophoresis.
Electrophoresis 2003;24(3):363-9.
2003: Adel M Abushoffa; Marianne Fillet; Anne-Catherine Servais; Ph Hubert; Jacques Crommen
Enhancement of selectivity and resolution in the enantioseparation of uncharged compounds using mixtures of oppositely charged cyclodextrins in capillary electrophoresis.
Electrophoresis 2003;24(3):343-50.
2002: Patrice Chiap; O Rbeida; B Christiaens; Ph Hubert; Dieter Lubda; KS Boos; Jacques Crommen
Use of a novel cation-exchange restricted-access material for automated sample clean-up prior to the determination of basic drugs in plasma by liquid chromatography.
Journal of chromatography. A 2002;975(1):145-55.
2002: Adel M Abushoffa; Marianne Fillet; Ph Hubert; Jacques Crommen
Prediction of selectivity for enantiomeric separations of uncharged compounds by capillary electrophoresis involving dual cyclodextrin systems.
Journal of chromatography. A 2002;948(1-2):321-9.
2002: Patrice Chiap; Ph Hubert; Jacques Crommen
Strategy for the development of automated methods involving dialysis and trace enrichment as on-line sample preparation for the determination of basic drugs in plasma by liquid chromatography.
Journal of chromatography. A 2002;948(1-2):151-61.
2002: Patrice Chiap; Attilio Ceccato; R Gora; Ph Hubert; Joseph Géczy; Jacques Crommen
Automated determination of pirlindole enantiomers in plasma by on-line coupling of a pre-column packed with restricted access material to a chiral liquid chromatographic column.
Journal of pharmaceutical and biomedical analysis 2002;27(3-4):447-55.
2002: Charles Kabengera; Patricia Bodart; Ph Hubert; Leopold Thunus; Alfred Noirfalise
Optimization and validation of arsenic determination in foods by hydride generation flame atomic absorption spectrometry.
Journal of AOAC International 2002;85(1):122-7.
2001: B Toussaint; M Palmer; Patrice Chiap; Ph Hubert; Jacques Crommen
On-line coupling of partial filling-capillary zone electrophoresis with mass spectrometry for the separation of clenbuterol enantiomers.
Electrophoresis 2001;22(7):1363-72.
2001: Patrice Chiap; Attilio Ceccato; B Miralles Buraglia; Bruno Boulanger; Ph Hubert; Jacques Crommen
Development and validation of an automated method for the liquid chromatographic determination of sotalol in plasma using dialysis and trace enrichment on a cation-exchange pre-column as on-line sample preparation.
Journal of pharmaceutical and biomedical analysis 2001;24(5-6):801-14.
2000: Patricia Bodart; C Kabengera; Alfred Noirfalise; Ph Hubert; Luc Angenot
Determination of alpha-solanine and alpha-chaconine in potatoes by high-performance thin-layer chromatography/densitometry.
Journal of AOAC International 2000;83(6):1468-73.
2000: B Toussaint; Bruno Streel; Attilio Ceccato; Ph Hubert; Jacques Crommen
Determination of the enantiomers of 3-tert.-butylamino-1,2-propanediol by high-performance liquid chromatography using mass spectrometric detection.
Journal of chromatography. A 2000;896(1-2):201-7.
2000: B Toussaint; C Pitti; Bruno Streel; Attilio Ceccato; Ph Hubert; Jacques Crommen
Quantitative analysis of N-acetylcysteine and its pharmacopeial impurities in a pharmaceutical formulation by liquid chromatography-UV detection-mass spectrometry.
Journal of chromatography. A 2000;896(1-2):191-9.
2000: B Toussaint; A L Duchateau; S van der Wal; A Albert; Ph Hubert; Jacques Crommen
Comparative evaluation of four detectors in the high-performance liquid chromatographic analysis of chiral nonaromatic alcohols.
Journal of chromatographic science 2000;38(10):450-7.
2000: B Toussaint; A L Duchateau; S van der Wal; A Albert; Ph Hubert; Jacques Crommen
Determination of the enantiomers of 3-tert.-butylamino-1,2-propanediol by high-performance liquid chromatography coupled to evaporative light scattering detection.
Journal of chromatography. A 2000;890(2):239-49.
2000: Bruno Streel; Ph Hubert; Attilio Ceccato
Determination of fenofibric acid in human plasma using automated solid-phase extraction coupled to liquid chromatography.
Journal of chromatography. B, Biomedical sciences and applications 2000;742(2):391-400.
2000: Marianne Fillet; Ph Hubert; Jacques Crommen
Enantiomeric separations of drugs using mixtures of charged and neutral cyclodextrins.
Journal of chromatography. A 2000;875(1-2):123-34.
2000: Patrice Chiap; B M Buraglia; Attilio Ceccato; Ph Hubert; Jacques Crommen
Automated liquid chromatographic determination of atenolol in plasma using dialysis and trace enrichment on a cation-exchange precolumn for sample handling.
Journal of chromatography. B, Biomedical sciences and applications 2000;739(1):205-17.
2000: B Toussaint; Ph Hubert; Ubbo R Tjaden; Jan van der Greef; Jacques Crommen
Enantiomeric separation of clenbuterol by transient isotachophoresis-capillary zone electrophoresis-UV detection new optimization technique for transient isotachophoresis.
Journal of chromatography. A 2000;871(1-2):173-80.
2000: Patrice Chiap; Brigitte Evrard; M A Bimazubute; Pascal de Tullio; Ph Hubert; Luc Delattre; Jacques Crommen
Determination of albendazole and its main metabolites in ovine plasma by liquid chromatography with dialysis as an integrated sample preparation technique.
Journal of chromatography. A 2000;870(1-2):121-34.
2000: B Toussaint; J Gysler; Ph Hubert; Ubbo R Tjaden; Jan van der Greef; Jacques Crommen
In-line concentration and enantioseparation of clenbuterol by transient isotachophoresis-capillary zone electrophoresis-UV detection.
Biomedical chromatography : BMC 2000;14(1):32-3.
2000: L Fotsing; B Boulanger; Patrice Chiap; Marianne Fillet; Ph Hubert; Jacques Crommen
Multivariate optimization approach for the separation of water-soluble vitamins and related compounds by capillary electrophoresis.
Biomedical chromatography : BMC 2000;14(1):10-1.
1999: L Fotsing; Marianne Fillet; Patrice Chiap; Ph Hubert; Jacques Crommen
Elimination of adsorption effects in the analysis of water-soluble vitamins in pharmaceutical formulations by capillary electrophoresis.
Journal of chromatography. A 1999;853(1-2):391-401.
1999: Attilio Ceccato; B Toussaint; Patrice Chiap; Ph Hubert; Jacques Crommen
Automated sample preparation techniques for the determination of drug enantiomers in biological fluids using liquid chromatography with chiral stationary phases.
Enantiomer 1999;4(3-4):305-15.
1998: Attilio Ceccato; Ph Hubert; Pascal de Tullio; Jean-François Liégeois; A Felikidis; Joseph Géczy; Jacques Crommen
Enantiomeric separation of pirlindole by liquid chromatography using different types of chiral stationary phases.
Journal of pharmaceutical and biomedical analysis 1998;18(4-5):605-14.
1998: Marianne Fillet; Ph Hubert; Jacques Crommen
Method development strategies for the enantioseparation of drugs by capillary electrophoresis using cyclodextrins as chiral additives.
Electrophoresis 1998;19(16-17):2834-40.
1998: Attilio Ceccato; Bruno Boulanger; Patrice Chiap; Ph Hubert; Jacques Crommen
Simultaneous determination of methylphenobarbital enantiomers and phenobarbital in human plasma by on-line coupling of an achiral precolumn to a chiral liquid chromatographic column.
Journal of chromatography. A 1998;819(1-2):143-53.
1998: Attilio Ceccato; Ph Hubert; Pascal de Tullio; Jean-François Liégeois; M Stachow; Joseph Géczy; Jacques Crommen
Simultaneous determination of pirlindole enantiomers and dehydropirlindole by chiral liquid chromatography.
Journal of pharmaceutical and biomedical analysis 1998;17(6-7):1071-9.
1998: Marianne Fillet; L Fotsing; G Schomburg; Ph Hubert; Jacques Crommen
Enantioseparation of acidic drugs by capillary electrophoresis using dual systems with mixtures of charged and neutral cyclodextrins.
Biomedical chromatography : BMC 1998;12(3):131-2.
1997: Attilio Ceccato; Patrice Chiap; Ph Hubert; Jacques Crommen
Automated determination of tramadol enantiomers in human plasma using solid-phase extraction in combination with chiral liquid chromatography.
Journal of chromatography. B, Biomedical sciences and applications 1997;698(1-2):161-70.
1997: Attilio Ceccato; B Toussaint; Patrice Chiap; Ph Hubert; Jacques Crommen
Enantioselective determination of oxprenolol in human plasma using dialysis coupled on-line to reversed-phase chiral liquid chromatography.
Journal of pharmaceutical and biomedical analysis 1997;15(9-10):1365-74.
1997: Marianne Fillet; Ph Hubert; Jacques Crommen
Enantioseparation of nonsteroidal anti-inflammatory drugs by capillary electrophoresis using mixtures of anionic and uncharged beta-cyclodextrins as chiral additives.
Electrophoresis 1997;18(6):1013-8.
1997: L Fotsing; Marianne Fillet; I Bechet; Ph Hubert; Jacques Crommen
Determination of six water-soluble vitamins in a pharmaceutical formulation by capillary electrophoresis.
Journal of pharmaceutical and biomedical analysis 1997;15(8):1113-23.
1997: Ph Hubert; V Hurlet; Jean-Michel Rigo; Paul Coucke; Gustave Moonen; Jacques Crommen
Fluorescence detection of a neurotoxic astroglia-released factor using gradient liquid chromatography after precolumn derivatization.
Biomedical chromatography : BMC 1997;11(2):93-5.
1996: Attilio Ceccato; Patrice Chiap; Ph Hubert; B Toussaint; Jacques Crommen
Automated determination of verapamil and norverapamil in human plasma with on-line coupling of dialysis to high-performance liquid chromatography and fluorometric detection.
Journal of chromatography. A 1996;750(1-2):351-60.
1996: Marianne Fillet; I Bechet; Ph Hubert; Jacques Crommen
Resolution improvement by use of carboxymethyl-beta-cyclodextrin as chiral additive for the enantiomeric separation of basic drugs by capillary electrophoresis.
Journal of pharmaceutical and biomedical analysis 1996;14(8-10):1107-14.
1995: I Bechet; Marianne Fillet; Ph Hubert; Jacques Crommen
Quantitative analysis of non-steroidal anti-inflammatory drugs by capillary zone electrophoresis.
Journal of pharmaceutical and biomedical analysis 1995;13(4-5):497-503.
1994: I Bechet; Marianne Fillet; Ph Hubert; Jacques Crommen
Determination of benzodiazepines by micellar electrokinetic chromatography.
Electrophoresis 1994;15(10):1316-21.
1994: I Bechet; P Paques; Marianne Fillet; Ph Hubert; Jacques Crommen
Chiral separation of basic drugs by capillary zone electrophoresis with cyclodextrin additives.
Electrophoresis 1994;15(6):818-23.
1994: Ph Hubert; Patrice Chiap; M Moors; B Bourguignon; D L Massart; Jacques Crommen
Knowledge-based system for the automated solid-phase extraction of basic drugs from plasma coupled with their liquid chromatographic determination. Application to the biodetermination of beta-receptor blocking agents.
Journal of chromatography. A 1994;665(1):87-99.
1993: Ph Hubert; Patrice Chiap; Brigitte Evrard; Luc Delattre; Jacques Crommen
Fully automated determination of sulfamethazine in ovine plasma using solid-phase extraction on disposable cartridges and liquid chromatography.
Journal of chromatography 1993;622(1):53-60.
1992: I Bechet; Attilio Ceccato; Ph Hubert; P Herné; Jacques Crommen
Determination of meprobamate in pharmaceutical dosage forms also containing carbromal by liquid chromatography and indirect photometric detection.
Journal of pharmaceutical and biomedical analysis 1992;10(10-12):995-9.
1992: Ph Hubert; Patrice Chiap; Attilio Ceccato; I Bechet; R Sibenaler-Dechamps; P Maes; Jacques Crommen
Determination of verapamil and norverapamil in human plasma by liquid chromatography: comparison between a liquid-liquid extraction procedure and an automated liquid-solid extraction method for sample preparation.
Journal of pharmaceutical and biomedical analysis 1992;10(10-12):937-42.
1991: Ph Hubert; Patrice Chiap; Jacques Crommen
Automatic determination of diltiazem and desacetyldiltiazem in human plasma using liquid-solid extraction on disposable cartridges coupled to HPLC--Part II: Optimization of liquid-solid extraction.
Journal of pharmaceutical and biomedical analysis 1991;9(10-12):883-7.
1991: Ph Hubert; Patrice Chiap; Jacques Crommen
Automatic determination of diltiazem and desacetyldiltiazem in human plasma using liquid-solid extraction on disposable cartridges coupled to HPLC--Part I: Optimization of the HPLC system and method validation.
Journal of pharmaceutical and biomedical analysis 1991;9(10-12):877-82.
1989: Ph Hubert; M Renson; Jacques Crommen
A fully automated high-performance liquid chromatographic method for the determination of indomethacin in plasma.
Journal of pharmaceutical and biomedical analysis 1989;7(12):1819-27.